One-dimensional Tb3+-doped beta-Ga2O3 nanofibers were prepared by a simple and cost-effective electrospinning process. Field emission scanning electron microscopy (FE-SEM). X-ray diffraction (XRD), Raman technique, and photoluminescence (PL) were used to characterize the electrospun nanofibers. FE-SEM results indicated that the diameters all of the nanofibers ranged from 100 to 300 nm, and the lengths of nanofibers reached up to several millimeters. The XRD and Raman results showed that the Ga2O3 phase belongs to the monoclinic phase. Under ultraviolet excitation, the beta-Ga2O3:Tb3+ samples showed green emission with the strongest peak at 550 nm, corresponding to D-5(4) -> F-7(5) transition of Tb3+ ions. The luminescence intensity had been further studied as a function of the doping concentration of Tb3+ in the beta-Ga2O3 samples. (C) 2011 Elsevier B.V. All rights reserved.